Crystallization provides an energy efficient separation process.
Xylene exists in the form of three isomers:
1,2 dimethylbenzene
(ortho-Xylene)
1,3 dimethylbenzene (meta-Xylene) Download our brochure
1,4
dimethylbenzene (para-Xylene) Download our brochure
There are many uses for
solutions of mixed Xylene isomers including solvent in the printing, rubber,
electronics and leather industries. The most commercially important product is
the 1,4 isomer (p-Xylene) since it is used as a feedstock in the production of
terephthalic acid, which is a monomer used in the production of the polymer
(PET) widely used in the production of bottles, films and fibers.
Due
to their similar boiling points it is difficult to completely separate the
Xylene isomers by distillation. The most common technique used today is
adsorption. This occurs when one isomer is preferentially attracted to an
adsorbent. The mixed isomer solution is pumped through a column that is loaded
with a specially developed resin that will become loaded with the para-Xylene
isomer. After a period of time the adsorbent is flushed to extract the
para-Xylene and so provides an increase in the purity of the para-isomer.
Repeating this process will provide high purity para-Xylene.

The low viscosity and rapid crystal growth in para-xylene purification systems allow use of the high capacity screw type wash columns.
Melt crystallization can also be used to effectively separate the mixed
Xylenes. This accounts for 25-30% of the world’s production of para-Xylene. The
melting temperature of the pure para- isomer is much higher (+13°C) than the
ortho- (-25 °C) or meta- (-48°C) isomers. It is possible to form high purity
para-Xylene crystals in mixed Xylene solutions even down to its eutectic
(±13wt% para-Xylene). When this solid is separated from the remaining liquid
high purity para-Xylene can be recovered.
A hybrid system utilizing
adsorption and crystallization can provide high purity para-Xylene and is an
energy efficient method to expand the capacity of existing adsorption systems.