The typical configuration for a suspension based melt crystallization
system is shown in the schematic. Crude product is cooled in scraped surface
crystallizers. These may be exchanger type or vessel type crystallizers
depending on the specific application. The crystallizer produces pure product
crystals and thus concentrates the impurities in the remaining liquid mother
liquor. The crystals are then separated from the impurity rich mother liquor
producing a pure product stream and a reject stream. The reject contains the
concentrated impurities but also valuable product which may be recovered
depending on the specific application.
Each individual crystal is
suspended in the mother liquor and is allowed to grow free flowing in the
liquid. With billions of crystals per cubic meter the growth surface can reach
5,000 to 10,000 m² per m³ of volume. This massive growth surface allows near
ideal growth rates that result in the characteristic pure crystals expected
from the eutectic crystallization process.
Since all of the impurities
are now in the mother liquor it is most important to remove all of this liquid
from the outside of the crystals. The crystallizer suspension is pumped into a
wash column where the pure crystals are separated and then washed to remove any
remaining mother liquor. The efficient washing action provided in the wash
column is unmatched by any other solid/liquid separation device. The pure
product crystals are then melted and discharged from the system.
Suspension based crystallizers produce pure crystals. Wash columns can
effectively remove all of the mother liquor and thereby produce ultra high
purity product.
- Proven technology
More than 100 wash columns installed worldwide
- Industrial applications
Capacities ranging from 10 kg/h up to 50,000
kg/h product
- Growing acceptance
Crystallization technologies are rapidly maturing
- Product development
Pilot scale equipment is available to demonstrate
the technology on an industrially relevant scale
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